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FLAME
Update for PSEM to version 4.6.1 (1.80 MB)
FLAME Update for Windows to version 4.6.1 (1.80 MB)
What's new in SLICE version 2.0.6 for Windows
This version may require you to update your current
database after backing it up, by running "DB Updater.exe" (included
in the download). The data stored in your database is not altered, but
additional columns will be added to the database for the additional properties
added in this release.
- Fixed a few bugs and improved the overall stability.
- Added the ability to import spectra with known chemistries in oxide
percent.
A checkbox was added to the User preferences, that when checked, modifies
the input to accomodate the chemistries properly. There should be an
element
list that includes the atomic numbers of all elements certified (or
known).
The Sample type should be listed as known or certified, and the category
should be listed as minerals, clay, etc. A typical partial input is
as follows:
#ELEMENTS : 8,11,12,13,14,20,22,24,25,26
##CATEGORY : minerals
##SAMPLETYPE : certified
each element with its atomic number and oxide concentration should be
listed:
##QUANT : 11, 0.12
##QUANT : 12, 9.43.
The oxygen concentration needs not and should not be entered.
Alternatively, the chemistries, etc., can be edited after importing,
by first
changing the category to minerals, the sample type to known or certified,
etc,
and executing a quant. This will add the oxide percent, and oxide formula
columns to the elements tab, and they can be edited normally by adding
the
known oxide chemistries as listed in the NIST certified specs, etc.The
oxide
formula's can also be edited if necessary.
- Fixed a bug which prevented importing spectra in certain cases;
- Fixed a few small bugs discovered during final testing
- Update Database" has been added to the main menu. However it
will not
update the current (opened) database. It will only allow you to select
another
database for updating (If you are currently in SLICE, the current database
is
already updated).
- When the target of a query is an XRF spectrum, or if the detector
has a
beryllium window, the "Search" page automatically sets the
"Best Fit"
parameters to "Selected Range" and sets appropriate upper
and lower limits
for the search. They, of course, can be overwritten, but they at least
suggest
optimized conditions.
- When starting a Search, if nothing is checked in the "Use Source"
group, the
background color for the group box is highlighted in Cyan, and the Source
type
of the unknown spectrum is highlighted in red, suggesting that the appropriate
check box should be checked. If nothing is checked, the search will
look
through the entire database, adding to the time and uncertainties
- Similarly, SLICE will suggest items to be checked under "Search
Options".
Ignoring the suggestions will usually increase the search times, and
increase
the uncertainties.
- The main menu item "Check Database" has been replaced with
"Populate
Database". which is more descriptive of the action taken. When
a database is
updated, spaces are created to contain additional parameters and metadata.
Populate Database' fills in these spaces, so that spectra can be queried
more
efficiently.
- On import, the file is scanned for the presence of "TUBE",
or "TUBEKV", or if
the "SIGNALTYPE" (source) is listed as "EDS/XRF",
SLICE assumes the
spectrum is from an XRF system.
- The "Known Weight %" column has been added to XRF spectra
(since SLICE
currently does not calculate chemical compositions other than "Relative
%").
If the Material Type is specified as "known", "certified"
or "nominal", the
column is created and remains as long as the Material Type remains as
above.
- If the spectrum source is SEM or TEM, and the Material Type is specified
as
"known", "certified" or "nominal", the
column is created and remains as long
as the Material Type remains as above. The known chemistries are also
imported for these souce types.
- It is now possible to Search XRF spectra based on compositions of
either
"Known Weight %" or "Relative %", and also to Tabulate
"Known Weight %"
and "Relative %" from XRF spectra.
- Export as EMSA File" has been updated to handle additional XRF
parameters
and to export the current element list, as well as a list of elements
and "known"
chemistries, when the Material Type is specified as "known",
"certified" or
"nominal" as above. The element list and known chemistries
are exported (if
available) for SEM/TEM spectra as well.
- Check Zero Offset"has been removed from the main menu.
- Modified to collect directly from a system with PulseTor detector
and electronics.
- Modified User Preferences.
- Updated report to reflect more of the recently added parameters.
- Expanded the number of files that can be "batch edited"
in the Spectrum Explorer from 500 to 1000.
- Fixed a problem that occurred when "batch editing" spectra
from the Spectrum Explorer.
- Search has been modified to fully utilize the additional xrf parameters.
- SLICE has been updated to allow additional XRF parameters to be stored
with the database. If the xray incidence angle (typically -135 degrees)
is included, and the statistics adequate, the Compton Scatter peaks
are properly labeled.
- SLICE is now able to recognize the HASP and runs properly under Windows
VISTA.
- Fixed a problem which caused some windows to be distorted when running
under Windows XP or Windows VISTA.
- The "Search" page has been redesigned to be more compact
and efficient and to permit expansion of SLICE to other spectroscopies.
- Added the ability to supress summary results when they are below a
user defined minimum.
- The "SLICE Preferences" page has also been redesigned for
the same reasons.
- "Check Database" will search out and correct some potential
problems in the database (e.g. missing data).
- The "Search" page will now suggest upper and lower search
limits when appropriate (e.g. when the unknown spectrum is from xrf,
or is from a detector with a Be window).
- The Overlap and Summary pages were modified to eliminate potential
problems.
- In cases where spectra are from a TEM or XRF instrumrnt, The grid
or tube are automatically added to the qualitative analysis, but fully
ignored for the quantitative analysis
- Source has been changed from "tem" to "TEM/EDS",
from "xrf" to "XRF/EDS", and from "sem"
or "micro" to "SEM/EDS" for consistency..
- An additional line has been added to the "Database Properties"
form to report the number of spectra that are not of the above types.
- Properties can now be tabulated, and the statistics displayed for
those that are strictly numeric.
- When printing the Overlap window (after a Search), if the "Add
Report" item (new item) in the PopUp Menu is checked, the printout
is formatted into a report in which all items relating to the query
are listed. The laboratory, analyst, date and sample name are a prominent
part of the report. The analyst and laboratory, are obtained from the
"User Preferences" (Cntrl+U), If they have not been entered,
the info is derived from the properties of the top spectrum in the spectrum
list (usually the "Unknown").
- Added the capability (for those systems that can collect spectra directly)
to collect a spectrum relative to a displayed reference spectrum, chosen
from the spectra contained in the database.
- Modified the "Intelli-Search" rules to aid the users, by
defaulting to more practical values, based on the last 6 years of use
with mixed spectra.
- Modified the Spectrum Explorer and added "Source" to the
"View By" list, making it possible to easily observe spectra
collected only by XRF/EDS (xrf), SEM/EDS (micro), or TEM/EDS (tem).
- "Classified" has been added to the Classification menu..
- The "Properties Info - Notes section has been modified to allow
opening URLs (if any are present & if there is an internet connection),
by clicking in the Notes tab.
- Radiopacity has been added to the properties in the SLICE database.
It can be included in Searches, tabulations, etc.
- "Dental" has been added to the "Material Category"
menus on the Search page and the "Import Template" page.
- The oxide indication has been added to the results header, and Search
has been modified to change the drop-down menu from elements to oxides
- The peak ID sensitivity has been modified, so as to allow smaller
peaks to be identified and labeled
- The main window and explorer window have been modifed so as to note
more succinctly when an image is missing, that should be present, as
reported in the database
- Oxide concentration has been added to SLICE for materials corresponding
to the following requirements. The spectrum must be from a mineral,
glass, clay, sand, soil, meteorite, or concrete, and must contain oxygen.
PeakID or quant will add an "Oxide" column in the Elements
Tab, which will contain the oxide formulas corresponding to the oxide
analysis. Default oxide formulas are inserted, but may be edited ( e.g.
Fe2O3 instead of FeO). The quant results may change to reflect the composition
of the new oxide formula. Clicking in the column headers will cause
the element display to cycle from Weight, to Atomic, to Oxide to Relative
percent.
- Other modifications were made to eliminate software bugs, or to increase
stability
What's new
in FLAME
version 4.6.1 for Windows
- Disabled Analysis->Preferences->Oxide
check box if Window Type is anything but Beryllium. (All versions)
- Corrected export
of EMSA Window types. (All versions)
- Corrected a situation
which could have prevented quantitative analysis with Match if the standard's
chi-square was too large. (All versions)
- Modified FLAME
so that when "Verify" is selected, the regions that contain the element
peaks of interest are drawn in Cyan, the reconstructed spectrum is in
red, and the raw spectrum is in yellow. Appropriate legends are also
displayed. (All versions)
- Trimmed the quantitative
output for better column alignment. (All versions)
- Updated the TIFF
import to properly handle both PSEM 75 and PSEM 2000 software. We have
found that in many cases, the TIFFs do not contain all the information
required by FLAME. We therefore insert reasonable values for those parameters
(e.g. live time). We suggest that you examine the Spectrum Info after
import to see if in fact, the parameters are reasonable and correct.
If not, edit them before going on. (All versions)
- Added the ability
to turn off the TIFF import warnings (for batch imports). (All versions)
- Disabled all but
NotePad under Word Processor. (All versions)
- Modified File->Open...
to remember the last location and file type opened ( *.prf, *.fdb, or
*.ems/sp). (All versions)
- Modified to open
EMSA files independent of line terminator (or lack of line terminator).
(All versions)
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Last updated: March 4, 2011
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